New nitrogen-containing peroxide oligomers (NPO) were synthesized via interaction of copolymers of maleic anhydride with either hydroxyl or secondary amine functionalities of the low molecular weight peroxide modifiers. The virgin oligomers as well asthe peroxide products acquired on their basis were characterized by active oxygen contents, elemental analysis, intrinsic viscosity values, thin-layer chromatography, and H1 NMR spectra. Kinetic features and mechanism of styrene polymerization initiated by NPO were studied and the process was shown to correspond to a typical radical polymerization process. NPO are suspected to be of interest for diverse interface modification applications.

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