The photosensibilized anionic mechanism of homopolymerization of ED-20 epoxy oligomer and its copolymerization with butylmethacrylate in the presence of dry triethylamine is shown on the basis of experimental data. The intermediate product of ED-20 photohomopolymerization forming a liquid epoxyoligomeric compound with end hydroxyl and ionic groups on HCl treatment is isolated. The identification of the intermediate hydroxyl-containing oligomer, photohomopolymer, and photocopolymer is carried out by means of IR spectroscopy and other methods.

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