This paper presents the results of investigation of phase-structural state, magneto-optical and magneto-resistive properties of multilayer spin-valve films structures on the basis of Fe, Co and Au. It was found that annealing of the samples up to T_a = 600 - 720 K leads to the formation of limited solid solution (s.s.) (Au, Co(Fe)) based on fcc-Au that considerably influences on the magnetic properties of the systems. The conditions and formation procedure of the most heat-stable systems with maximum values of magneto resistance, sensitivity to magnetic field changes and induction of demagnetization were found.

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